By Brian M. Tissue
Chapter 1 Making Measurements (pages 1–52):
Chapter 2 pattern training, Extractions, and Chromatography (pages 53–102):
Chapter three Classical tools (pages 103–140):
Chapter four Molecular Spectroscopy (pages 141–175):
Chapter five Acid?Base Equilibria and task (pages 177–220):
Chapter 6 Buffer options and Polyprotic Acids (pages 221–244):
Chapter 7 Complexation and Precipitation Equilibria (pages 245–291):
Chapter eight Electroanalytical Chemistry (pages 293–339):
Chapter nine Atomic Spectrometry (pages 340–366):
Chapter 10 Analytical Separations (pages 367–406):
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Extra info for Basics of Analytical Chemistry and Chemical Equilibria
1 M nitric acid solution for analysis by atomic absorption spectrometry. (a) drinking water (this one should be easy). (b) chicken livers (organic components might complex some of the metal). (c) a geologic mineral (must be digested in a ﬂux at high temperature— possible loss of analyte owing to volatilization). 10. For the Pb analyses in the previous exercise, discuss the relative pros and cons of using a calibration curve versus standard addition to calibrate the measurement. Calculational Practice For the following spreadsheet exercises, title the top of the worksheet with the exercise number, your name, and date.
Volumetric glassware will have a tolerance etched on the surface and usually a label such as TD (to deliver) or TC (to contain). “TD” means that you let the liquid drain and you do not blow out any residual liquid. “TC” is found on volumetric ﬂasks and some pipettes, which are designed for preparing but not delivering a calibrated amount. Volumetric glassware is available as Class A and Class B, with the manufacturing tolerance for Class B being twice as large as for Class A. 05 ml. 01 ml. 10 Volumetric glassware.
Check that you get the same result as the Q-test calculation above. 5 CALIBRATION The preceding section described the statistical tools to describe the repeatability of replicate measurements. Calibration is the process of measuring a known quantity to determine the relationship between the measurement signal and the analyte amount or concentration. Calibration allows the analyst to estimate the accuracy of a measurement, procedure, or instrument. Calibration is critical to GLP and method development and validation.
Basics of Analytical Chemistry and Chemical Equilibria by Brian M. Tissue