By Steven D. Burke, Rick L. Danheiser
Recognising the serious want for bringing a convenient reference paintings that offers with the preferred reagents in synthesis to the laboratory of working towards natural chemists, the Editors of the acclaimed Encyclopedia of Reagents for natural Synthesis (EROS) have chosen an important and precious reagents hired in modern natural synthesis.
guide of Reagents for natural Synthesis: Oxidizing and decreasing brokers, presents the artificial chemist with a handy compendium of knowledge focusing on an important and regularly hired reagents for the oxidation and relief of natural compounds, extracted and up-to-date from EROS. The inclusion of a bibliography of experiences and monographs, a compilation of natural Syntheses tactics with proven experimental information and references to oxidizing and lowering brokers will make sure that this instruction manual is either entire and handy.
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Extra info for Handbook of reagents for organic synthesis
Eco,, (10) C1 98% ee (s) 55% ee 0 p BY t ,k,COzEt (6) R =Me, 50%, 98% ee R = Et, 64%. 19 The pheromone (R)-(+)-hexadecanolide has been prepared in this way by reduction of the corresponding 6-keto acid (eq 7 1 . ~ ~ Acyloin Condensations. ~~ r / OH (12) overall 25% 85-95% ee Cyclization of Squalene-like Substrates. 29 BY (8) PhOCO OH % ’ PhOCO OH 99% ee BY Activated Double-Bond Hydrogenation. Fermenting BY is able to carry out the hydrogenation of double bonds which bear certain functional groups.
D. Bull. SOC. Chirn. Rorn. 1929, 11, 37 (CA 1930, 24, 110). 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16. 17. 18. 19. 20. 21. 22. 23. 24, 25, 26. 27. 28. 29. 30. 31. Turner, A. ; Ringold, H. J. JCS(C) 1967, 1720. Mathew, T. S. TL 1990,31,4497. Kulkami, M. ; Matsushita, H. BCJ 1988,61, 3283. ; Sano, K. JOC 1979,44, 2647. Aurich, H. ; Mobus, K. D. T 1989,45,5815. ; Vasisht, S. ; Meyers, R. CB 1980,113,2916. ; Schaumberg,J. ; Duffel, M. ; Rosazza, J. P. JOC 1987, 52, 1500. Current, S . P. JOC 1983,48, 1779.
JCS(PI) 1990, 3 199. 43. ; Ishikawa, N. CL 1984, 1815. 44. Rao, K. V. ; Sampath Kumar, H. M. TL 1991, 32, 6611. 10) c 6 b o 2 (useful as an oxidizing' or dehydrogenation agent;' can function as a dienophile3 in the Diels-Alder reaction or as a dipolarophile to prepare 5-hydroxyindole derivatives4) Alternate Name: p-benzoquinone. 318g~m-~. Solubility: slightly sol water; sol alcohol, ether, hot petroleum ether, and aqueous base. Form Supplied in: yellowish powder; widely available. Handling, Storage, and Precautions: the solid has an irritating odor and can cause conjunctivitis, corneal ulceration, and dermatitis.
Handbook of reagents for organic synthesis by Steven D. Burke, Rick L. Danheiser