HPLC Methods for Recently Approved Pharmaceuticals - download pdf or read online

By George Lunn

ISBN-10: 0471669415

ISBN-13: 9780471669418

An fundamental source for busy researchersYour time is valuable-too priceless to spend looking during the technical literature looking for the proper HPLC assay recommendations in your initiatives. With HPLC equipment for lately licensed prescription drugs, you are going to speedy determine and mirror the proper systems in your undertaking wishes, with no need to consult unique resource guides. extra of a while can then be spent within the lab, no longer the library.Covering the suitable global literature via 2003, this ebook selections up the place Dr. Lunn's acclaimed HPLC equipment for Pharmaceutical research left off. It hands you with verified HPLC assay concepts for enormous quantities of newly authorized medications, in addition to medicinal drugs for which assay equipment have been just recently constructed. Combining special descriptions of tactics with in particular annotated references, this functional instruction manual offers you:* HPLC equipment for 390 in general prescribed pharmaceutical compounds* a number of approaches for every drug indexed together-making it effortless to mix 'n match for custom designed ways* equipment for medicines in organic fluids and for bulk and formulated medicines* Chemical constructions, molecular weights and formulation, and CAS Registry Numbers* Cross-references to The Merck Index* Retention instances of alternative medicinal drugs that may be assayed utilizing an analogous equipment

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Okayama et al. Chem. 1990, 36, 1494. ; Horiguchi, S. Health, 1994, 36, 49–56. L. , 1999, 27, 432–435. ; Tieckelmann, H. , 1986, 375, 57–63. W. , 1990, 527, 134–139. ; Kajiwara, M. , 1992, 40, 1948–1950. M. , 1979, 185, 605–611. ; Wolf, U. , 1985, 149, 29–34. I. Acta, 1986, 161, 11–18. ; Okayama, A. B, 1994, 654, 165–169. Okayama, A. , 1988, 426, 365–369. ; Miura, R. , 1990, 36, 1494–1497. ; Hasegawa, T. , 1987, 33, 1665–1667. 64 CAS Registry No: 161814-49-9 Merck Index: 13, 594 O O N H N OH S O CH3 CH3 SAMPLE Matrix: blood Sample preparation: Condition a C18 SPE cartridge (Baker) with 3 mL MeOH and 3 mL water.

1998, 139 (Suppl. 52), 8–11. 1% trifluoroacetic acid in MeCN. Evaporate the supernatant to dryness under reduced pressure at room temperature. 5 sodium acetate, vortex, centrifuge. 0 potassium phosphate buffer containing 5 mM tetrabutylammonium hydrogen phosphate, inject a 50 µL aliquot. 6 Zorbax RX-C18 Column temperature: 35 Mobile phase: Gradient. 0 potassium phosphate buffer containing 5 mM tetrabutylammonium hydrogen phosphate 2:98. 0 potassium phosphate buffer containing 5 mM tetrabutylammonium hydrogen phosphate 65:35.

Okayama et al. Chem. 1990, 36, 1494. ; Horiguchi, S. Health, 1994, 36, 49–56. L. , 1999, 27, 432–435. ; Tieckelmann, H. , 1986, 375, 57–63. W. , 1990, 527, 134–139. ; Kajiwara, M. , 1992, 40, 1948–1950. M. , 1979, 185, 605–611. ; Wolf, U. , 1985, 149, 29–34. I. Acta, 1986, 161, 11–18. ; Okayama, A. B, 1994, 654, 165–169. Okayama, A. , 1988, 426, 365–369. ; Miura, R. , 1990, 36, 1494–1497. ; Hasegawa, T. , 1987, 33, 1665–1667. 64 CAS Registry No: 161814-49-9 Merck Index: 13, 594 O O N H N OH S O CH3 CH3 SAMPLE Matrix: blood Sample preparation: Condition a C18 SPE cartridge (Baker) with 3 mL MeOH and 3 mL water.

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